An Agilent GCMSD (low resolution, single quadrupole mass spectrometer) fitted with a Headspace module is used to perform trace level analysis of residual solvents from the synthesis process. Both polar and non-polar GC columns can be used. Unknown compounds in a mixture can be identified using the NIST library of spectra. This instrument is ideal for quantitating known compounds in a complex mixtures. The mass range is limited to 800 Daltons.
The requester will provide a list of solvents and approximately 15 mg of solid sample for this analysis.